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Procedure – Powder/Chip Samples

Prepare the instrument as outlined in the operator's instruction manual.

Determine the instrument blank.

Login a minimum of three Blank reps.

Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open. Insert a *** Nickel Capsule (leave capsule open) into the open port at top of loading head.

Note: samples using automation should be placed in the appropriate autoloader position before starting the analysis sequence. Once the sequence has started, the automatic analysis will start and end automatically.

装有自动旁路阀的可快速拆装氧水捕集装置。美国分析仪厂家供应

Sample Preparation

Typically, titanium and zirconium samples are chemically etched to remove surface contamination when oxygen and nitrogen are determined. However, etching can introduce hydrogen into the sample.

ASTM method E 1409 "Determination of Oxygen and Nitrogen in Titanium and Titanium Alloys by the Inert

Gas Fusion Technique", as updated in 1996, permits either etching or abrading (filing) of the test specimen.

ASTM E 1447 "Determination of Hydrogen in Titanium and Titanium Alloys by the Inert Gas Fusion Thermal

Conductivity/Infrared Detection Method" permits surface preparation by abrading (if necessary to remove

contamination). Differences in sample preparation present somewhat of a dilemma regarding simultaneous

determination of O, N, and H in titanium. However, abrading samples with a file to remove surface

contamination will yield accurate O, N, and H results. The ONH836 utilizes a high-power electrode furnace to quickly and efficiently release the target gases from within the sample, which allows for a very rapid simultaneous determination of oxygen, nitrogen, and hydrogen.

湖南美国LECO分析仪厂家报价工具条、滑动条和下拉式菜单简化了校正和数据处理的参数设定。

736 Series: Oxygen/Nitrogen by Inert Gas Fusion

The 736 family of Elemental Analyzers is designed for routine measurement of oxygen and nitrogen content of

inorganic materials, ferrous and nonferrous alloys, andrefractory materials using the inert gas fusion technique.

These instruments feature our Cornerstone brand ® software, a custom interface designed specifically for

touch-screen operation. Developed by combining longterm research with customer feedback, this easy-to-use

software gives you complete access to instrument control, analysis settings, diagnostics, reporting, and more—without sacrificing valuable bench space.

Oxygen, Nitrogen, and Hydrogen in Refractory Metals

Summary

Oxygen and nitrogen are alloying elements in titanium, and are also classified as alpha stabilizing elements as they promote alpha phase alloys. Interstitial oxygen and nitrogen levels can be used to regulate the tensile strength of the material, but due to its high solubility can cause unwanted surface embrittlement. This phenomenon can be leveraged,however, under controlled processing to create surface films that increase surface hardness and wear properties.

改进的红外检测池技术。

力可ONH836氧氮氢分析仪

特点和优势

国际**的非色散红外及热导检测器 ，无移动部件，不需要手动调整

采用三个**的红外器检测氧含量，同时检测CO和CO2，然后在转化为CO2集中检测，原理上是**完善的，所以不仅可以保证中间量程的测量精度，在**含量和高含量的检测范围内同样可以满足精度要求

高性能的红外检测器配置***恒温绝热技术，消除了外界环境温度的干扰

长寿命的红外发射光源和无漂移的电路设计保证检测器的长期稳定性

力可**的动态流量补偿控制DFC系统，保证了流量系统的完善，可以精确控制整个气路中的流量，保持流量恒定**改善了材料中氮分析的准确度

可以旁路的OMI-2 气路强化过滤装置增强了检测器的稳定性，使得分析结果更加准确

可选自动功能

20位试样自动进样系统

通用下电极坩埚支座，容纳各种坩埚使用

无需人工干预的全自动清扫系统

20位或100位全自动分析系统。湖南美国LECO分析仪厂家报价

全自动分析系统（可选） 。美国分析仪厂家供应

Procedure - Solid Samples

Instrument calibration/drift correction.

Add approximately 0.05 g of *** Graphite Powder to a *** Graphite Crucible.

Firmly place the crucible on the lower electrode tip or appropriate autoloader position.

Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and end automatically.

Repeat steps 3b through 3j a minimum of three times for each calibration/drift standard used.

Calibrate/drift following the procedure outlined in the operator's instruction manual.

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